Complete Elemental Analysis
- Duration: 3 days for live courses
- Experience level: Intermediate
- Delivery methods: Face-to-face | Offsite training & consultancy | Online | Onsite training & consultancy | Tailored training |
- Type of course: Universal
- Applicable to manufacturer(s): Agilent | Thermo |
- CPD Approved: Not yet approved
- Scheduled course price: £1,200.00 + TAX per delegate
- Course discounts: RSC HEaTED Cambridge Network CAMS members receive a discount on this course
Your complete guide to elemental analysis
Learn everything you need to know about elemental analysis, with this 3-day classroom-based training for professionals, students and chemists. This complete analytical chemistry course combines the intermediate Practical Essentials of Elemental Analysis with the more advanced Elemental Analysis Clinic, to provide complete training, enabling you to understand your elemental analysis instrumentation, develop methods, maintain and troubleshoot them. Alongside diagrams, animations and examples from different industries, improve your understanding further with the opportunity to handle (see, in virtual courses) elemental analysis instrument parts and consumables such as an MS quadrupole, ICP torch, nebulisers and peristaltic pump.
This course covers all the practical theory you need to know about elemental analysis and its related techniques including (AAS), inductively coupled plasma optical emission spectroscopy (ICP-OES) and inductively coupled plasma mass spectrometry (ICP-MS) from both the chemistry and physical perspectives, covering the instrument modules from autosamplers for automated sampling and sample preparation through to data analysis. This course also looks at how to choose the elemental analysis techniques for an application, set-up the instrument, develop & optimise the methods and then finally how to maintain & troubleshoot the instrumentation.
Why should I join?
At the end of this course, you will have a complete understanding of elemental analysis techniques and, be able to confidently apply all aspects studied on this course to your own laboratory and analytical work.
This Complete Elemental Analysis course gives you:
- A complete understanding of the instrumentation used in elemental analysis from the sample preparation, through to the PC for data analysis
- Clear insights and explanations into AAS and ICP components such as the burner, nebulisers, spray chambers and peristaltic pumps
- Understanding of basic data analysis from understanding calibration graphs to generating data reports
- Familiarity with spectrometers and detectors in elemental analysis
- A solid understanding of elemental analysis method development, alongside maintenance and troubleshooting common problems
What would I learn?
This intermediate to advanced level course will provide all-round understanding, covering the practical theory of elemental analysis you will learn the:
- Importance of good sample preparation in elemental analysis including microwave digestion and the use of organic solvents
- How sample introduction varies between each technique of AAS, ICP-OES and ICP-MS
- Distinctive types of detectors available in elemental analysis from photomultiplier tubes (PMT) to charge coupled device (CCD)
- Different types of optics and gratings available in AAS and ICP-OES including monochromators, polychromators, diffraction and Echelle gratings
- Discover the different mass spectrometers that can be hyphenated to ICP from single quadrupoles (SQMS) to magnetic sector MS
- Common sampling techniques used for elemental analysis, including various acids available for use, as well as the use of hot blocks and microwave digestors for extraction
- How to develop elemental analysis methods then put into practice with a classroom-based exercise
- Develop a solid understanding of elemental analysis maintenance and troubleshooting and put into practice with exercises examining chromatograms to identify and solve problems
What knowledge will I gain?
By the end of the course, you will:
- Have complete knowledge of the chemical and physical principles and concepts of elemental analysis
- Comprehend how to choose the sample introduction system, and the pros and cons of various nebuliser and spray chamber types for ICP-OES and ICP-MS
- Know how sample preparation and matrix matching standards are pivotal to elemental analysis
- Understand the many types of interferences that can occur in elemental analysis, including spectral interferences, physical interferences and isobaric interferences
- Know the differences between high resolution (HRMS) and tandem (MS/MS) mass spectrometry and the different mass analysers such as Time of Flight (ToFMS) and multi-collector ICP-MS
- Be familiar with the principles of atomic absorption, atomic emission and ionisation
- Grasp both qualitative and quantitative data analysis processes for AAS, ICP-OES and ICP-MS
- Know the strategy for developing a robust elemental analysis method, how to monitor the method performance and prepare the method for validation
- Understand common maintenance required on elemental analysis instrumentation, including checking and replacing pump tubing, cleaning of sampler cones and skimmer cones and how to maintain an ICP torch and nebuliser
- Understand how to troubleshoot common issues with elemental analysis systems, examining frequent problem as such as, autosampler issues, nebuliser problems, and sensitivity losses and how to troubleshoot contamination that could come from various sources
Is this course for me?
This training is designed for anyone with basic knowledge who would like to take this to a higher level and learn the full extent of elemental analysis instrumentation and applications, including:
- Laboratory analysts & technicians wanting clear, structured, in-depth training or a refresher on these techniques
- Laboratory or line managers overseeing elemental analysis and instruments
- Data analysts and report writers who interpret results but do not use the instruments
- Service and consultant engineers who need a chemistry-focused viewpoint
- Sales, marketing, or commercial teams working with elemental analysis systems, consumables, data, or laboratory services who would like a complete, in-depth perspective
If elemental analysis touches your work in any way, this well-planned course delivered by experts in the field equips you to understand the science behind these techniques.
This course includes
- Practical Essentials of Elemental Analysis
- Practical Essentials of Elemental Analysis introduction, sample preparation, sample introduction, spectrometers for ICP-OES and AAS
- Practical Essentials introduction to Elemental Analysis
- Practical Essentials of Elemental Analysis sample preparation techniques, collection, and storage
- Practical Essentials of Elemental Analysis sample introduction
- Practical Essentials of Elemental Analysis spectrometers and detectors for AAS and ICP-OES
- Practical Essentials of Elemental Analysis spectrometers, detectors, mass spectrometers, and data analysis
- The Elemental Analysis Clinic